(L) ASTM E260–85, Standard Practice for Packed Column Gas Chromatography, incorporated by reference for s. NR 664.1063. _Hlk167104422(m) ASTM E681-09, Standard Test Method for Concentration Limits of Flammability of Chemicals (Vapors and gases), incorporated by reference for s. NR 661.0021 (1). _Hlk167105874(n) ASTM D323-20, Standard Test Method for Vapor Pressure of Petroleum Products, (Reid Method), incorporated by reference for s. NR 661.0021 (1). (o) ASTM D140-70, Standard Practice for Sampling Bituminous Materials, incorporated by reference for ch. NR 661 Appendix I. (p) ASTM D346-75, Standard Practice for Collection and Preparation of Coke Samples for Laboratory Analysis, incorporated by reference for ch. NR 661 Appendix I. (q) ASTM D420-69, Guide to Site Characterization for Engineering, Design, and Construction Purposes, incorporated by reference for ch. NR 661 Appendix I. (r) ASTM D1452-65, Standard Practice for Soil Investigation and Sampling by Auger Borings, incorporated by reference for ch. NR 661 Appendix I. (s) ASTM D2234-76, Standard Practice for Collection of a Gross Sample of Coal, incorporated by reference for ch. NR 661 Appendix I. (t) ASTM D2879-86, Standard Test Method for Vapor Pressure—Temperature Relationship and Initial Decomposition Temperature of Liquids by Isoteniscope, incorporated by reference for ch. NR 664 and subch. BB of ch. NR 665. (u) ASTM G21-70 (1984a), Standard Practice for Determining Resistance of Synthetic Polymer Materials to Fungi, incorporated by reference for ch. NR 664 and subch. N of ch. NR 665. (v) ASTM G22-76 (1984b), Standard Practice for Determining Resistance of Plastics to Bacteria, incorporated by reference for ch. NR 664 and subch. N of ch. NR 665. (3) The following materials are available for purchase from the National Technical Information Service, 5285 Port Royal Road, Springfield, VA 22161; or for purchase from the Superintendent of Documents, U.S. Government Printing Office, Washington, DC 20402, (202) 512–1800:
(b) Screening Procedures for Estimating the Air Quality Impact of Stationary Sources, Revised, October 1992, EPA Publication EPA–450/R–92–019, incorporated by reference for ch. NR 666 Appendix IX. (c) The following methods as published in the test methods compendium known as “Test Methods for Evaluating Solid Waste, Physical/Chemical Methods,” EPA Publication SW–846, Third Edition:
1. Method 0011, Revision 1, August 2018, incorporated by reference for ch. NR 666 Appendix IX. 7. Method 1010B, December 2018, incorporated by reference for s. NR 661.0021. 8. Method 1020C, December 2018, incorporated by reference for s. NR 661.0021. 9. Method 1110A, November 2004 and Update IIIB, incorporated by reference for s. NR 661.0022. _Hlk14852236211. Method 1330A, Extraction Procedure for Oily Wastes, dated July 1992 and in Update I, incorporated by reference for ch. NR 661 Appendix IX. 12. Method 9010C, dated November 2004 and Update IIIB, incorporated by reference for ss. NR 668.40, 668.44, and 668.48. 13. Method 9012B, November 2004 and Update IIIB, incorporated by reference for ss. NR 668.40, 668.44, and 668.48. 14. Method 9040C, November 2004 and Update IIIB, incorporated by reference for s. NR 661.0022. 16. Method 9071B, n-Hexane Extractable Material (HEM) for Sludge, Sediment, and Solid Samples, dated April 1998 and in Update IIIA, incorporated by reference for ch. NR 661 Appendix IX. Note: A suffix of “A” in the method number indicates revision one (the method has been revised once). A suffix of “B” in the method number indicates revision two (the method has been revised twice). A suffix of “C” in the method number indicates revision three (the method has been revised three times). A suffix of “D” in the method number indicates revision four (the method has been revised four times).
(4) The following materials are available for purchase from the National Fire Protection Association, 1 Batterymarch Park, P.O. Box 9101, Quincy, MA 02269–9101, (800) 344-3555, www.nfpa.org/.: (5) The following materials are available for purchase from the Organization for Economic Co-operation and Development, Environment Directorate, 2 rue André Pascal, F-75775 Paris Cedex 16, France, www.oecd-ilibrary.org/: (a) Guidance Manual for the Control of Transboundary Movements of Recoverable Wastes, copyright 2009, Annex B: OECD Consolidated List of Wastes Subject to the Green Control Procedure and Annex C: OECD Consolidated List of Wastes Subject to the Amber Control Procedure, incorporated by reference for ss. NR 662.082 (1), 662.083 (2), (4), and (7), and 662.084 (2) and (4). (6) The following materials are available for purchase from the American Petroleum Institute, 1220 L Street, Northwest, Washington, DC 20005:
(a) American Petroleum Institute Publication 2517, Third Edition, February 1989, Evaporative Loss from External Floating-Roof Tanks, incorporated by reference for s. NR 665.1084. _Hlk170821092(b) American Petroleum Institute Publication, Guide for Inspection of Refinery Equipment, Chapter XIII, “Atmospheric and Low-Pressure Storage Tanks,” 4th edition, 1981, incorporated by reference for s. NR 661.0191 (2). (7) The following materials are available for purchase from the Steel Tank Institute, 944 Donata Court, Lake Zurich, IL 60047:
(a) Steel Tank Institute, “Standard for Dual Wall Underground Storage Tanks,” 2006, incorporated by reference for s. NR 661.0193 (4). _Hlk144983980NR 661.0021 (1) (a) It is a liquid, other than an aqueous a solution containing less than 24 percent alcohol by volume and at least 50 percent water by weight, and that has a flash point less than 60° C 60 degrees Celsius or 140° F140 degrees Fahrenheit, as determined by a Pensky-Martens Closed Cup Tester, using the test method specified in ASTM Standard D 93-79 or D 93-80, incorporated by reference in s. NR 660.11, or a Setaflash Closed Cup Tester, using the test method specified in ASTM Standard D 3278-78 using one of the following ASTM standards: ASTM D93-79, D93-80, D3278-78, D8174-18, or D8175-18 as specified in SW-846 Test Methods 1010B or 1020C, incorporated by reference in under s. NR 660.11. 4Section 4 NR 661.0021 (1) (c) and (d) are repealed and recreated to read: NR 661.0021 (1) (c) It is an ignitable compressed gas. An ignitable compressed gas is a gas with all of the following characteristics:
1. A compressed gas is a material or mixture having in the container an absolute pressure exceeding 40 pounds per square inch at 70 degrees Fahrenheit or, regardless of the pressure at 70 degrees Fahrenheit, having an absolute pressure exceeding 104 p.s.i. at 130 degrees Fahrenheit; or a liquid flammable material having a vapor pressure exceeding 40 p.s.i. absolute at 100 degrees Fahrenheit as determined by ASTM Test D323-20.
2. A compressed gas shall be characterized as ignitable if any one of the following occurs:
a. Either a mixture of 13 percent or less, by volume, with air forms a flammable mixture or the flammable range with air is wider than 12 percent, regardless of the lower limit. These limits shall be determined at atmospheric temperature and pressure. The method of sampling and test procedure shall be the ASTM E681-09, incorporated by reference under s. NR 660.11, or other equivalent methods approved by the associate administrator of the pipeline and hazardous materials safety administration in the U.S. department of transportation. (d) It is an oxidizer. An oxidizer for the purpose of this subchapter is a substance that yields oxygen readily to stimulate the combustion of organic matter, for example, a chlorate, permanganate, inorganic peroxide, or a nitrate. An oxidizer is any of the following:
1. An organic compound containing the bivalent -O-O- structure and that may be considered a derivative of hydrogen peroxide when one or more of the hydrogen atoms have been replaced by organic radicals shall be classed as an organic peroxide unless it has any of the following characteristics:
a. The material meets the definition of a division 1.1, 1.2, or 1.3 explosive under s. NR 661.0023 (1) (h), in which case it shall be classed as an explosive. c. It is determined that the predominant hazard of the material containing an organic peroxide is other than that of an organic peroxide.
d. According to data on file with the pipeline and hazardous materials safety administration in the U.S. department of transportation, it has been determined that the material does not present a hazard in transportation.
5Section 5 Effective Date. This rule takes effect on the first day of the month following publication in the Wisconsin Administrative Register as provided in s. 227.22 (2) (intro.), Stats. 6Section 6 Board adoption. This rule was approved and adopted by the State of Wisconsin Natural Resources Board on September 25, 2024. Dated at Madison, Wisconsin _____________________________.
STATE OF WISCONSIN
DEPARTMENT OF NATURAL RESOURCES
BY ______________________________________
For Karen Hyun, Ph.D., Secretary
