Table 6 Fuel Analysis Requirements |
To conduct a fuel analysis for the following pollutant... | You shall… | Using…a |
1. Mercury | a. Collect fuel samples | Procedure in s. NR 462.05 (4) (c) or ASTM D2234/D2234M−03e1 D2234/D2234M-20 (for coal), or ASTM D6323−98 (2003) (for biomass) or equivalent. |
c. Prepare composited fuel samples | SW−846−3050B (for solid samples) or SW−846−3020A (for liquid samples) or ASTM D2013−01D2013/D2013M-21 (for coal), or ASTM D5198−92 (2003) (for biomass) or equivalent. |
e. Determine moisture content of the fuel type | ASTM D3173−02D3173/D3173M-17a, or ASTM E871−82 (1998) or equivalent. |
2. Total selected metals | a. Collect fuel samples | Procedure in s. NR 462.05 (4) (c) or ASTM D2234/D2234M−03e1 D2234/D2234M-20 (for coal), or ASTM D6323−98 (2003) (for biomass) or equivalent. |
c. Prepare composited fuel samples | SW−846−3050B (for solid samples) or SW−846−3020A (for liquid samples) or ASTM D2013−01D2013/D2013M-21 (for coal), or ASTM D5198−92 (2003) (for biomass) or equivalent. |
e. Determine moisture content of the fuel type | ASTM D3173−02D3173/D3173M-17a or ASTM E871−82 (1998) or equivalent. |
3. Hydrogen chloride | a. Collect fuel samples | Procedure in s. NR 462.05 (4) (c) or ASTM D2234/D2234M−03e1 D2234/D2234M-20 (for coal) or ASTM D6323−98 (2003) (for biomass) or equivalent. |
c. Prepare composited fuel samples | SW−846−3050B (for solid samples) or SW−846−3020A (for liquid samples) or ASTM D2013−01D2013/D2013M-21 (for coal) or ASTM D5198−92 (2003) (for biomass) or equivalent. |
e. Determine moisture content of the fuel type | ASTM D3173−02D3173/D3173M-17a or ASTM E871−82 (1998) or equivalent. |
Table 2 |
CFR Appendix References |
CFR Appendix Referenced | Title | Incorporated by Reference For |
(9e) (9m) (9s) | 40 CFR part 51 Appendix M, Method 201 40 CFR part 51 Appendix M, Method 201A 40 CFR part 51 Appendix M, Method 202 | Determination of PM10 Emissions Determination of PM10 and PM2.5 Emissions from Stationary Sources Dry Impinger Method for Determining Condensable Particulate Emissions from Stationary Sources | NR 439.06 (1m) NR 439.06 (1m) NR 439.06 (1) NR 439.06 (1m) |
(14m) | 40 CFR part 60 Appendix A, Method 3C | Determination of Carbon Dioxide, Methane, Nitrogen, and Oxygen form Stationary Sources | NR 439.07 (8) (a) 1. NR 439.07 (8) (b) 5. |
(20c) | 40 CFR part 60 Appendix A, Method 29 | Determination of Metals from Stationary Sources | NR 439.06 (5) |
(20v) | 40 CFR part 60 Appendix A, Method 320 | Measurement of Vapor Phase Organic and Inorganic Emissions by Extractive Fourier Transform Infrared (FTIR) Spectroscopy | NR 439.06 (2) (a) NR 439.06 (3) (a) NR 439.06 (6) (a) NR 439.07 (8) (e) |
Table 2 |
CFR Appendix References |
(21m) | 40 CFR part 60 Appendix F | Quality Assurance Procedures | NR 428.23 (1) (b) 2. c. NR 439.06 (2) (b) NR 439.06(4)(b) NR 439.06(6)(b) NR 439.06(7)(b) NR 439.06 (9) (a) 2. NR 439.07(8)(b)4. NR. 439.09(1)-(4), (7)-(7r), (7v) NR 439.095 (6) NR 466.10 (2) NR 466.24 (2) (d) 1. b. |
Table 5 ASTM Standard References |
Standard Number | Standard Title | Incorporated by Reference For |
(3) | ASTM D129-00 (2005) | Standard Test Method for Sulfur in Petroleum Products (General Bomb Method) | 40 CFR part 60 Appendix A, Method 19 40 CFR part 75 Appendices A and D NR 439.08 (2) (b) |
(4) | ASTM D240-02 D240-19 | Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter | 40 CFR part 60 Appendix A, Method 19 40 CFR part 75 Appendices A, D, E, and F NR 400.02 (79) NR 439.08 (2) (c) |
(25) (26) | ASTM D1552-03D1552-23 ASTM D1826−94 (1998)(2017) | Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) Standard Test Method for Calorific Value of Gases in Natural Gas Range by Continuous Recording Calorimeter | 40 CFR part 75 Appendices A and D NR 439.08 (2) (b) 40 CFR part 60 Appendix A, Method 19 40 CFR part 75 Appendices E and F NR 400.02 (79) |
(30) | ASTM D2013-01D2013/D2013M-21 | Standard Method of Preparing Coal Samples for Analysis | 40 CFR part 60 Appendix A, Method 19 40 CFR part 75 Appendix F NR 439.08 (1) (b) NR 462, Table 6 |
(33) | ASTM D2234/D2234M- 03e1D2234/D2234M-20 | Standard Practice for Collection of a Gross Sample of Coal | 40 CFR part 60 Appendix A, Method 19 40 CFR part 75 Appendix F NR 439.08 (1) (a) NR 439.085 (2) (a) 1. NR 439.085 (2) (b) 1. NR 439.085 (2) (c) 1. NR 462, Table 6 |
(41m) | ASTM D3172-89 (2002) D3172-13(2021)e1 | Standard Practice for Proximate Analysis of Coal and Coke | NR 439.098 (1) (b) |
(42) | ASTM D3173-02 D3173/D3173M-17a | Standard Test Method for Moisture in the Analysis Sample of Coal and Coke | 40 CFR part 60 Appendix A, Method 19 NR 439.08 (1) (f) NR 462, Table 6 |
(43) | ASTM D3174-04D3174-12(2018)e1 | Standard Test Method for Ash in the Analysis Sample of Coal and Coke from Coal | 40 CFR part 75 Appendix G NR 439.08 (1) (e) |
(44) | ASTM D3176-89 (2002)D3176-24 | Standard Practice for Ultimate Analysis of Coal and Coke | 40 CFR part 75 Appendices A and F NR 439.08 (1) (g) NR 439.098 (1) (a) |
Table 5 ASTM Standard References |
Standard Number | Standard Title | Incorporated by Reference For |
(47g) | ASTM D3302/D3302M-22a | Standard Test Method for Total Moisture in Coal | NR 439.08 (1) (f) |
Table 5 ASTM Standard References |
Standard Number | Standard Title | Incorporated by Reference For |
(51) | ASTM D4057-95 (2000)D4057-22 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products | 40 CFR part 75 Appendix D NR 439.08 (2) (a) |
(52) | ASTM D4177-95 (2000)D4177-22e1 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products | 40 CFR part 75 Appendix D NR 439.08 (2) (a) |
(53) | ASTM D4239-04aD4239-18e1 | Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High Temperature Tube Furnace Combustion Methods | 40 CFR part 60 Appendix A, Method 19 40 CFR part 75 Appendix A NR 439.08 (1) (c) |
(54) | ASTM D4294-03D4294-21 | Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy-Dispersive X-Ray Fluorescence Spectrometry | 40 CFR part 75 Appendices A and D NR 439.08 (2) (b) |
(55) | ASTM D4809-00D4809-18 | Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method) | 40 CFR part 75 Appendices D, E and F NR 439.08 (2) (c) NR 460.10 (2) (f) 2. |
(55g) | ASTM D5865-04D5865/D5865M-19 | Standard Test Method for Gross Calorific Value of Coal and Coke | NR 400.02 (79) NR 439.08 (1) (d) |
Table 5 ASTM Standard References |
Standard Number | Standard Title | Incorporated by Reference For |
(55r) | ASTM D6348-12 (2020) | Standard Test Method for Determination of Gaseous Compounds by Extractive Direct Interface Fourier Transform Infrared (FTIR) Spectroscopy | NR 439.06 (2) (a) NR 439.06 (3) (a) NR 439.06 (6) (a) NR 439.07 (8) (e) |