(i) ASTM E 260–85, Standard Practice for Packed Column Gas Chromatography, incorporated by reference for s. NR 664.1063. (j) ASTM E 926–88, Standard Test Methods for Preparing Refuse-Derived Fuel (RDF) Samples for Analyses of Metals, Test Method C—Bomb, Acid Digestion Method.
(k) ASTM D140-70, Standard Practice for Sampling Bituminous Materials, incorporated by reference for ch. NR 661, Appendix I. (L) ASTM D346-75, Standard Practice for Collection and Preparation of Coke Samples for Laboratory Analysis, incorporated by reference for ch. NR 661, Appendix I. (m) ASTM D420-69, Guide to Site Characterization for Engineering, Design, and Construction Purposes, incorporated by reference for ch. NR 661, Appendix I. (n) ASTM D1452-65, Standard Practice for Soil Investigation and Sampling by Auger Borings, incorporated by reference for ch. NR 661, Appendix I. (o) ASTM D2234-76, Standard Practice for Collection of a Gross Sample of Coal, incorporated by reference for ch. NR 661, Appendix I. (p) ASTM D2879-86, Standard Test Method for Vapor Pressure—Temperature Relationship and Initial Decomposition Temperature of Liquids by Isoteniscope, incorporated by reference for chs. NR 664 and 665, subch. BB. (q) ASTM G21-70 (1984a), Standard Practice for Determining Resistance of Synthetic Polymer Materials to Fungi, incorporated by reference for chs. NR 664 and 665, subch. N. (r) ASTM G22-76 (1984b), Standard Practice for Determining Resistance of Plastics to Bacteria, incorporated by reference for chs. NR 664 and 665, subch. N. (3) The following materials are available for purchase from the National Technical Information Service, 5285 Port Royal Road, Springfield, VA 22161; or for purchase from the Superintendent of Documents, U.S. Government Printing Office, Washington, DC 20402, (202) 512–1800.
(a) APTI Course 415: Control of Gaseous Emissions, EPA Publication EPA–450/2–81– 005, December 1981, incorporated by reference for ss. NR 664.1035, 665.1035, 670.024 and 670.025. (b) The following methods as published in the test methods compendium known as ‘‘Test Methods for Evaluating Solid Waste, Physical/Chemical Methods,’’ EPA Publication SW–846, Third Edition.
Note: A suffix of ‘‘A’’ in the method number indicates revision one (the method has been revised once). A suffix of ‘‘B’’ in the method number indicates revision two (the method has been revised twice). A suffix of ‘‘C’’ in the method number indicates revision three (the method has been revised three times). A suffix of ‘‘D” in the method number indicates revision four (the method has been revised four times).
1. Method 1311, September 1992, and Update I, incorporated by reference for ss. NR 661.24, 668.07 and 268.40. 2. Method 0011, December 1996, and Update III, incorporated by reference for ch. NR 666, Appendix IX. 3. Method 0023A, December 1996, and Update III, incorporated by reference for s. NR 666.104 and ch. NR 666, Appendix IX 4. Method 0050, December 1996, and Update III, incorporated by reference for s. NR 666.107 and ch. NR 666, Appendix IX. 5. Method 0051, December 1996 and Update III, incorporated by reference for s. NR 666.107 and ch. NR 666, Appendix IX. 6. Method 0060, December 1996, and Update III, incorporated by reference for s. NR 666.106 and ch. NR 666, Appendix IX. 7. Method 0061, December 1996 and Update III incorporated by reference for s. NR 666.106 and ch. NR 666, Appendix IX. 8. Method 1110A, November 2004 and Update IIIB, incorporated by reference for s. NR 661.22. 9. Method 9010C, dated November 2004 and Update IIIB, incorporated by reference for ss. NR 668.40, 668.44 and 668.48. 10. Method 9012B, November 2004 and Update IIIB, incorporated by reference for ss. NR 668.40, 668.44 and 668.48. 11. Method 9040C, November 2004 and Update IIIB, incorporated by reference for s. NR 661.22. (4) The following materials are available for purchase from the National Fire Protection Association, 1 Batterymarch Park, P.O. Box 9101, Quincy, MA 02269–9101.
(5) The following materials are available for purchase from the American Petroleum Institute, 1220 L Street, Northwest, Washington, DC 20005.
(a) API Publication 2517, Third Edition, February 1989, Evaporative Loss from External Floating-Roof Tanks, incorporated by reference for s. NR 665.1084. (6) The following materials are available for purchase from the Environmental Protection Agency, Research Triangle Park, NC.
(a) Screening Procedures for Estimating the Air Quality Impact of Stationary Sources, Revised, October 1992, EPA Publication No. EPA–450/R–92–019, incorporated by reference for ch. NR 666, Appendix IX. (7) The following materials are available for purchase from the Organisation for Economic Co-operation and Development, Environment Directorate, 2 rue Andre Pascal, 75775 Paris Cedex 16, France.
(a) OECD Green List of Wastes (revised May 1994), Amber List of Wastes and Red List of Wastes (both revised May 1993) as set forth in Appendix 3, Appendix 4 and Appendix 5, respectively, to the OECD Council Decision C (92)39/FINAL (Concerning the Control of Transfrontier Movements of Wastes Destined for Recovery Operations), incorporated by reference for s. NR 662.089. (8) The following Code of Federal Regulation Appendices are available for purchase from Superintendent of Documents, PO Box 371954, Pittsburgh, PA 15250-7954, (866) 512-1800.
(a) 40 CFR part 51, Appendix M, Method 204 Criteria for and Verification of a Permanent or Temporary Total Enclosure incorporated by reference for chs. NR 664, subch. CC and 665, subch. CC. (b) 40 CFR part 51, Appendix W Guideline on Air Quality Models (Revised), incorporated by reference for ch. NR 666, subch. H. (d) 40 CFR part 60, Appendix A, Methods 1 to 5 Various Titles, incorporated by reference for ch. NR 666, subch. H. (e) 40 CFR part 60, Appendix A, Method 1 Sample and Velocity Traverses for Stationary Sources , incorporated by reference for ch. NR 666, Appendix IX. (f) 40 CFR part 60, Appendix A, Method 2 Determination of Stack Gas Velocity and volumetric Flow Rate (Type S Pitot Tube) incorporated by reference for chs. NR 664, subch. AA and 665, subch. AA. (g) 40 CFR part 60, Appendix A, Method 2A Direct Measurement of Gas Volume through Pipes and Small Ducts, incorporated by reference for chs.NR 664, subch. AA and 665, subch. AA. (h) 40 CFR part 60, Appendix A, Method 2C Determination of Gas Velocity and Volumetric Flow Rate in Small Stacks or Ducts (Standard Pitot Tube) incorporated by reference for chs.NR 664, subch. AA and 665, subch. AA. (i) 40 CFR part 60, Appendix A, Method 2D Measurement of Gas Volume Flow Rates in Small Pipes and Ducts, incorporated by reference for chs.NR 664, subch. AA and 665, subch. AA. (j) 40 CFR part 60, Appendix A, Method 3 Gas Analysis for the Determination of Dry Molecular Weight, incorporated by reference for ch.NR 664, subch. O and ch. NR 666, Appendix IX (k) 40 CFR part 60, Appendix A, Method 3A, Determination of Oxygen and Carbon Dioxide Concentrations in Emissions from Stationary Sources (Instrumental Analyzer Procedure), incorporated by reference for ch. NR 666, Appendix IX (L) 40 CFR part 60, Appendix A, Method 10 Determination of Carbon Monoxide Emissions from Stationary Sources, incorporated by reference for ch. NR 666, Appendix IX. (m) 40 CFR part 60, Appendix A, Method 10A Determination of Carbon Monoxide Emissions in Certifying Continuous Emission Monitoring Systems at Petroleum Refineries, incorporated by reference for ch. NR 666, Appendix IX (n) 40 CFR part 60, Appendix A, Method 10B Determination of Carbon Monoxide Emissions from Stationary Sources, incorporated by reference for ch. NR 666, Appendix IX. (o) 40 CFR part 60, Appendix A, Method 18 Measurement of Gaseous Organic Compound Emissions by Gas Chromatography, incorporated by reference for chs.NR 664, subch. AA and 665, subch. AA. (p) 40 CFR part 60, Appendix A, Method 21 Determination of Volatile Organic Compounds Leaks, incorporated by reference for chs. NR 664, subchs. AA, BB and CC and 665, subchs. AA, BB and CC. (q) 40 CFR part 60, Appendix A, Method 22 Visual Determination of Fugitive Emissions from Material Sources and Smoke Emissions from Flares, incorporated by reference for chs. NR 664, subchs. AA and DD and 665, subchs. AA and DD. (r) 40 CFR part 60, Appendix A, Method 25D Determination of the Volatile Organic Concentration of Waste Samples, incorporated by reference for chs. NR 664, subch. CC and 665, subch. CC. (s) 40 CFR part 60, Appendix A, Method 25E Determination of Vapor Phase Organic concentration in Waste Samples, incorporated by reference for ch. NR 665, subch. CC. (t) 40 CFR part 60, Appendix A, Method 27 Determination of Vapor Tightness of Gasoline Delivery Tank using Pressure-Vacuum Test, incorporated by reference for ch. NR 664, subch. CC. (u) 40 CFR part 63, Appendix A, Method 301 Field Validation of Pollutant Measurement Methods from Various Waste Media, incorporated by reference for ch. NR 665, subch. CC. (v) 40 CFR part 63, Appendix C Determination of the Fraction Biodegraded (Fbio) in a Biological Treatment Unit, incorporated by reference for ch. NR 665, subch. CC. (w) 40 CFR part 63, Appendix D Alternative Validation Procedure for EPA Waste and Wastewater Methods, incorporated by reference for ch. NR 665, subch. CC. (x) 40 CFR part 136, Appendix A, Method 624 Purgeables, incorporated by reference for ch. NR 665, subch. CC. (y) 40 CFR part 136, Appendix A, Method 625 Base/Neutrals and Acids, incorporated by reference for ch. NR 665, subch. CC. (z) 40 CFR part 136, Appendix A, Method 1624 Volatile Organic Compounds by Isotope Dilution GC/MS, incorporated by reference for ch. NR 665, subch. CC. (za) 40 CFR part 136, Appendix A, Method 1625 Semivolatile Organic Compounds by Isotope Dilution GC/MS, incorporated by reference for ch. NR 665, subch. CC. SECTION 10. NR 660.31 (2) is amended to read:
NR 660.31 (2) The department may grant requests for a variance from classifying as a solid waste those materials that are reclaimed and then reused as feedstock within the original production process in which the materials were generated if the reclamation operation is an essential part of the production process. This determination will be based on all of the following criteria:
(a) How economically viable the production process would be if it were to use virgin materials, rather than reclaimed materials.
(b) The prevalence of the practice on an industry-wide basis.
(c) (b) The extent to which the material is handled before reclamation to minimize loss.
(d) (c) The time periods between generating the material and its reclamation, and between reclamation and return to the original primary production process.
(e) (d) The location of the reclamation operation in relation to the production process.
(f) (e) Whether the reclaimed material is used for the purpose for which it was originally produced when it is returned to the original process, and whether it is returned to the process in substantially its original form.
(g) (f) Whether the person who generates the material also reclaims it.
(h) (g) Other relevant factors.
SECTION 11. Chapter NR 661, Table of Contents, is repealed and recreated to read:
HAZARDOUS WASTE IDENTIFICATION AND LISTING
Subchapter A — General
NR 661.01 Purpose and scope.
NR 661.02 Definition of solid waste.
NR 661.03 Definition of hazardous waste.
NR 661.04 Exclusions.
NR 661.06 Requirements for recyclable materials.
NR 661.07 Residues of hazardous waste in empty containers.
NR 661.08 PCB wastes regulated under federal toxic substances control act.
NR 661.09 Requirements for universal waste.
